Abstract
In order to solve the problems of long time and poor accuracy in the determination of the solid content of accelerant, this paper proposed to use refractometer concentration testing technology to quickly determine the solid content of liquid accelerant. In addition, in order to study the accuracy of the determination method, accelerator samples with standard solid content, different solid contents, and different types were tested by the drying and weighing method and refractometer method, respectively. The results show that: ① for accelerator of the same standard, the discreteness of the test results by refractometer method is smaller, and the data is more stable. There is a better correlation with standard solid content; ② For the liquid accelerator with different solid contents, the correlation between the test results of the refractometer and standard solid content is better than that of the drying and weighing method, which can more accurately reflect the real solid content of liquid accelerator; ③ For the liquid accelerant with different solid contents, the test results of drying and weighing method and refractometer method have good linear correlation; ④ The refractometer method has good adaptability to the determination of solid content of different types/types of the accelerator, and the relative deviation between the modified results and the drying and weighing method is less than 0.8%.
Publication Date
6-18-2022
DOI
10.14048/j.issn.1671-2579.2022.03.045
First Page
251
Last Page
253
Submission Date
May 2025
Recommended Citation
YueE, Feng and Yongfeng, Wei
(2022)
"Study on Solid Content Measurement of Liquid Accelerator Based on Refractometer Method,"
Journal of China & Foreign Highway: Vol. 42:
Iss.
3, Article 45.
DOI: 10.14048/j.issn.1671-2579.2022.03.045
Available at:
https://zwgl1980.csust.edu.cn/journal/vol42/iss3/45
Reference
[1] 苏州混凝土水泥制品研究院有限公司. 混凝土外加剂匀质性试验方法:GB/T8077—2012[S]. 北京: 中国标准出版社, 2013. Suzhou Concrete & Cement Products Research Institute Co., Ltd. Methods for testing uniformity of concrete admixtures: GB/T 8077—2012S]. Beijing: Standards Press of China, 2013. [2] 马双平, 周芬, 朱华雄. 折射率法快测聚羧酸系减水剂含固量[J]. 建材世界, 2014, 35(3): 13-16+22. MA Shuangping, ZHOU Fen, ZHU Huaxiong. Determination of solid content of the polycarboxylate superplasticizer rapidly by measuring its refractive index[J]. The World of Building Materials, 2014, 35(3): 13-16+22. [3] 毛文. 阿贝折射仪检定(校准)中遇到的问题及解决方法[J]. 中国计量, 2010(1): 112-113. MAO Wen. Problems and solutions in verification (calibration) of abbe refractometers[J]. China Metrology, 2010(1): 112-113. [4] 王春辉. 阿贝折射仪测量结果的不确定度评定[J]. 计量与测试技术, 2008, 35(1): 3+5. WANG Chunhui. Evaluation of uncertainty in measurement of abbe refractometer[J]. Metrology & Measurement Technique, 2008, 35(1): 3+5. [5] 周丕炯.阿贝折射仪的光学原理[J].标准与检测,2001(4):56-57. ZHOU Pi-jiong. Optical principles of abbe refractometers[J].Standards and Testing, 2001(4): 56-57. [6] 王定兴, 徐丽红. 阿贝折射仪的消色散原理[J]. 物理实验, 1987, 7(5): 203-205+211. WANG Dingxing, XU Li-hong. Dispersion compensation principle in abbe refractometers [J]. Physics Experiments, 1987, 7(5): 203-205+211. [7] 王贤书, 王勤, 施建南. 折光率法测定薄荷醇溶液的组成[J]. 中国实用医药, 2008, 3(24): 84-85. WANG Xianshu, WANG Qin, SHI Jian-nan. Determination of menthol solution composition by refractometry [J]. China Practical Medicine, 2008, 3(24): 84-85.